DIN EN ISO 22959-2009 动植物油脂.在线受体络合物色谱法和荧光探测高效液相色谱法测定多环芳碳氢(ISO22959:2009),德文版本ENISO22959:2009
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【英文标准名称】:Animalandvegetablefatsandoils-Determinationofpolycyclicaromatichydrocarbonsbyon-linedonor-acceptorcomplexchromatographyandHPLCwithfluorescencedetection(ISO22959:2009);EnglishversionofDINENISO22959:2009-10
【原文标准名称】:动植物油脂.在线受体络合物色谱法和荧光探测高效液相色谱法测定多环芳碳氢(ISO22959:2009),德文版本ENISO22959:2009
【标准号】:DINENISO22959-2009
【标准状态】:现行
【国别】:德国
【发布日期】:2009-10
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:
【英文主题词】:Analysis;Animalfats;Animaloils;Coconutoil;Definitions;Determination;Determinationofcontent;Fats;Fluorimetry;Foodchemistry;Highperformanceliquidchromatography;HPLC;Hydrocarbons;Inter-laboratorytests;Liquidchromatography;Oils;Oliveoil;PAH;PAK;Polynucleararomatichydrocarbons;Soyabeanoil;Sunflowerseedoil;Testing;Testingdevices;Vegetablefats
【摘要】:ThisInternationalStandardspecifiesahighperformanceliquidchromatographic(HPLC)procedureforthedeterminationofpolycyclicaromatichydrocarbons(PAHs)inediblefatsandoils.Themethodhasbeenvalidatedforcoconut(CN),olive(OV),sunflower(SF),andsoybean(BO)oil,andispossiblyapplicabletootheroils,dependentonthedeterminationofappropriateparameters.ThelowestlevelofquantificationforthePAHsis0,1μg/kg.ThelowestpossibleamountofeachPAHwhichcanbedistinguishedfromthebaselinenoisehasnotbeendetermined.Thevalidatedconcentrationrangeofthemethodis0,1μg/kgto3,5IJg/kgforeachindividualPAH.Forsamplescontaining(light)PAHcontents:3,5μg/kg,dilutiontobringthecontentsintothevalidatedrangeispossible.Itisalsopossibletoadjusttherangeofthecalibrationcurves.However,rangesexceeding3,5μg/kghavenotbeenvalidated.PAHswhichcanbedeterminedbythismethodare:anthracene,phenanthrene,fluoranthene,pyrene,chrysene,benzo[a]anthracene,benzo[e]pyrene,benzo[a]pyrene,perylene,benzo[ghi]perylene,anthanthrene,dibenzo[a,h]anthracene,coronene,indeno[1,2,3-cd]pyrene,benzo[a]fluoranthene,benzo[b]fluoranthene,benzo[k]fluoranthene.
【中国标准分类号】:X14
【国际标准分类号】:67_200_10
【页数】:28P.;A4
【正文语种】:英语
【原文标准名称】:动植物油脂.在线受体络合物色谱法和荧光探测高效液相色谱法测定多环芳碳氢(ISO22959:2009),德文版本ENISO22959:2009
【标准号】:DINENISO22959-2009
【标准状态】:现行
【国别】:德国
【发布日期】:2009-10
【实施或试行日期】:
【发布单位】:德国标准化学会(DE-DIN)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:
【英文主题词】:Analysis;Animalfats;Animaloils;Coconutoil;Definitions;Determination;Determinationofcontent;Fats;Fluorimetry;Foodchemistry;Highperformanceliquidchromatography;HPLC;Hydrocarbons;Inter-laboratorytests;Liquidchromatography;Oils;Oliveoil;PAH;PAK;Polynucleararomatichydrocarbons;Soyabeanoil;Sunflowerseedoil;Testing;Testingdevices;Vegetablefats
【摘要】:ThisInternationalStandardspecifiesahighperformanceliquidchromatographic(HPLC)procedureforthedeterminationofpolycyclicaromatichydrocarbons(PAHs)inediblefatsandoils.Themethodhasbeenvalidatedforcoconut(CN),olive(OV),sunflower(SF),andsoybean(BO)oil,andispossiblyapplicabletootheroils,dependentonthedeterminationofappropriateparameters.ThelowestlevelofquantificationforthePAHsis0,1μg/kg.ThelowestpossibleamountofeachPAHwhichcanbedistinguishedfromthebaselinenoisehasnotbeendetermined.Thevalidatedconcentrationrangeofthemethodis0,1μg/kgto3,5IJg/kgforeachindividualPAH.Forsamplescontaining(light)PAHcontents:3,5μg/kg,dilutiontobringthecontentsintothevalidatedrangeispossible.Itisalsopossibletoadjusttherangeofthecalibrationcurves.However,rangesexceeding3,5μg/kghavenotbeenvalidated.PAHswhichcanbedeterminedbythismethodare:anthracene,phenanthrene,fluoranthene,pyrene,chrysene,benzo[a]anthracene,benzo[e]pyrene,benzo[a]pyrene,perylene,benzo[ghi]perylene,anthanthrene,dibenzo[a,h]anthracene,coronene,indeno[1,2,3-cd]pyrene,benzo[a]fluoranthene,benzo[b]fluoranthene,benzo[k]fluoranthene.
【中国标准分类号】:X14
【国际标准分类号】:67_200_10
【页数】:28P.;A4
【正文语种】:英语
下载地址: 点击此处下载
